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云南黄果冷杉的化学成分

常博, 肖琳婧, 张健, 赵守训, 叶文才, 殷志琦

常博, 肖琳婧, 张健, 赵守训, 叶文才, 殷志琦. 云南黄果冷杉的化学成分[J]. 中国药科大学学报, 2014, 45(1): 43-47. DOI: 10.11665/j.issn.1000-5048.20140107
引用本文: 常博, 肖琳婧, 张健, 赵守训, 叶文才, 殷志琦. 云南黄果冷杉的化学成分[J]. 中国药科大学学报, 2014, 45(1): 43-47. DOI: 10.11665/j.issn.1000-5048.20140107
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CHANG Bo, XIAO Linjing, ZHANG Jian, ZHAO Shouxun, YE Wencai, YIN Zhiqi. Chemical constituents from Abies ernestii var.salouenensis[J]. Journal of China Pharmaceutical University, 2014, 45(1): 43-47. DOI: 10.11665/j.issn.1000-5048.20140107
Citation: CHANG Bo, XIAO Linjing, ZHANG Jian, ZHAO Shouxun, YE Wencai, YIN Zhiqi. Chemical constituents from Abies ernestii var.salouenensis[J]. Journal of China Pharmaceutical University, 2014, 45(1): 43-47. DOI: 10.11665/j.issn.1000-5048.20140107
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云南黄果冷杉的化学成分

  • 1.

    中国药科大学天然药物化学教研室，天然药物活性组分与药效国家重点实验室

  • 2.

    江苏省中医药研究院转化医学实验室

  • 3.

    暨南大学中药及天然药物研究所，中药药效物质基础及创新药物研究广东省高校重点实验室

基金项目: 天然药物活性组分与药效国家重点实验室资助项目(No.ZJ11175)；国家自然科学基金资助项目(No.81001379)；江苏省第九批“六大人才高峰”高层次人才资助项目(No.2012-YY-008)；江苏省“青蓝工程”资助项目

Chemical constituents from Abies ernestii var.salouenensis

摘要

    摘要
  • 摘要: 采用硅胶、凝胶、反相柱色谱等各种色谱技术对云南黄果冷杉Abies ernestii var.salouenensis干燥枝叶80%乙醇提取物进行分离纯化，共得到13个化合物，根据理化数据对照及波谱学方法，分别鉴定为:(7S，8S)-3-甲氧基-3′，7-环氧-8，4′-氧化新木脂素-4，9，9′-三醇( 1 )，isomassonianoside B( 2 )，8，8′-二羟基松脂素( 3 )，莽草酸正丁酯( 4 )，对羟基苯甲酸( 5 )，莽草酸( 6 )，咖啡酸( 7 )，阿魏酸二十四醇酯( 8 )，苯甲酸( 9 )，芹菜素-8-C-α-L-鼠李糖-(1→2)-β-D-葡萄糖苷( 10 )，丁香亭-3-O-芸香糖苷( 11 )，5-羟基-3，4′，7-三甲氧基黄酮( 12 )，4′，5-二羟基-3，7-二甲氧基-6-甲基黄酮( 13 )。所有化合物均首次从该植物中分离得到，其中化合物 1~4 ， 6 ， 10~12 为首次从该属植物中分离得到。
    Abstract: Thirteen compounds were isolated from the branches and leaves of Abies ernestii var. salouenensis by silica gel, Sephadex LH-20 and ODS column chromatographies. Their structures were identified by physicochemical properties and spectral techniques as(7S, 8S)-3-methoxy-3′, 7-epoxy-8, 4′-oxyneoligna-4, 9, 9′-triol( 1 ), isomassonianoside B( 2 ), 8, 8′-dihydroxypinoresinol( 3 ), shikimic acid n-butyl ester( 4 ), 4-hydroxy benzoic acid( 5 ), shikimic acid( 6 ), caffeic acid( 7 ), hexacosyl ferulate( 8 ), benzoic acid( 9 ), apigenin-8-C-α-L-rhamnopyranosyl-(1→2)-β-D-glucopyranoside( 10 ), syringetin-3-O-rutinoside( 11 ), 5-hydroxy-3, 4′, 7-trimethoxyl flavone( 12 ), 4′, 5-dihydroxy-3, 7-dimethoxy-6-methyl flavone( 13 ). All compounds were isolated from this plant for the first time, and compounds 1 - 4 , 6 , 10 - 12 were isolated from this genus for the first time.
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  • [1] Delectis Florae Reipublicae Popularis Sinicae,Agendae Academiae sinicae Edita.Flora Reipublicae Popularis Sinicae(中国植物志)[M].Tomus 7.Beijing:Science Press,1978:93.
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  • 刊出日期:  2014-02-24

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