• 中国中文核心期刊
  • 中国科学引文数据库核心期刊
  • 中国科技核心期刊
  • 中国高校百佳科技期刊
高级检索

当归芍药散HPLC-DAD指纹图谱峰来源分析

胡虒尧, 周瑜, 陶春蕾, 宋欣, 许钒, 王运来

胡虒尧, 周瑜, 陶春蕾, 宋欣, 许钒, 王运来. 当归芍药散HPLC-DAD指纹图谱峰来源分析[J]. 中国药科大学学报, 2014, 45(2): 205-209. DOI: 10.11665/j.issn.1000-5048.20140213
引用本文: 胡虒尧, 周瑜, 陶春蕾, 宋欣, 许钒, 王运来. 当归芍药散HPLC-DAD指纹图谱峰来源分析[J]. 中国药科大学学报, 2014, 45(2): 205-209. DOI: 10.11665/j.issn.1000-5048.20140213
HU Siyao, ZHOU Yu, TAO Chunlei, SONG Xin, XU Fan, WANG Yunlai. HPLC-DAD fingerprint of Danggui-Shaoyao-San and its synergy[J]. Journal of China Pharmaceutical University, 2014, 45(2): 205-209. DOI: 10.11665/j.issn.1000-5048.20140213
Citation: HU Siyao, ZHOU Yu, TAO Chunlei, SONG Xin, XU Fan, WANG Yunlai. HPLC-DAD fingerprint of Danggui-Shaoyao-San and its synergy[J]. Journal of China Pharmaceutical University, 2014, 45(2): 205-209. DOI: 10.11665/j.issn.1000-5048.20140213

当归芍药散HPLC-DAD指纹图谱峰来源分析

基金项目: 国家自然科学基金资助项目(No.81173368)

HPLC-DAD fingerprint of Danggui-Shaoyao-San and its synergy

  • 摘要: 建立了当归芍药散的HPLC-DAD指纹图谱分析方法,确定了部分特征峰的归属。采用高效液相色谱法,色谱柱为Welchrom C18柱(250 mm×4.6 mm,5 μm);流动相为乙腈-0.05%磷酸水溶液(梯度洗脱),检测波长为230 nm,流速为1 mL/min。从建立的当归芍药散指纹图谱中,对照出当归芍药散中的21个特征峰8个来自当归,11个来自白芍,13个来自川芎,4个来自白术,2个来自茯苓,3个来自泽泻,同时鉴定出7个峰的化学结构。当归芍药散指纹图谱的结果为鉴别当归芍药散的质量提供了依据,也为阐明各部位的药效物质基础提供了参考。
    Abstract: An HPLC-DAD fingerprint method was developed for the simultaneous determination of Danggui-Shaoyao-San. A Welchrom C18 column(250 mm×4. 6 mm, 5 μm)was used with a gradient mobile phase system of acetonitrile-water containing 0. 05% phosphoric acid. The detection wavelength was 230 nm; the flow rate was 1 mL/min. From the fingerprint we can conclude that in the total 21 peaks, 8 was from Angelicae sinensis, 11 from Paeonia lactiflora, 13 from the Ligustici Chuanxiong, 4 from Atractylodis macrocephalae, 2 from Poria cocos, and 3 from Rhizoma Alismatis. The validated method was applied to the quality control of Danggui-Shaoyao-San, providing a basis for the efficacy of various parts to clarify the material basis.
  • [1] Yi L,Qi LW,Li P,et al.Simultaneous determination of bioactive constituents in Danggui Buxue Tang for quality control by HPLC coupled with a diode array detector,an evaporative light scattering detector and mass spectrometry[J].Anal Biol Chem,2007,389(2):571-580.
    [2] Liu HM,Liu J,Li KY.RP-HPLC simultaneous determination of ferulic acid and paeoniflorin in angelica and peony[J].Chin Tradit Pat Med(中成药),2007,29(11):1 707-1 707.
    [3] Wang B,Han G,Zhang XJ,et al.Content changes of glycyrrhizin between single and mixed decoction of Dahuang-Gancao decoction[J].Chin Tradit Pat Med(中成药),2010,32(10):1 794-1 796.
    [4] Wang R,Zhan XR,Wang J,et al.Study in contents of paeoniflorin in Radix Paeoniae alba individual boiling extracts and Guizhi decoction co-boiling extracts[J].J Shanxi Colg Tradit Chin Med(山西中医学院学报),2011,12(3):23-25.
    [5] Yi X,Huang YC,Wei G.Research on the influence of various compatibility on fingerprint of Yupingfeng decoction by HPLC[J].Chin J Exp Tradit Med Form(中国实验方剂学杂志),2009,15(3):1-3.
    [6] Zhu W,Qiu XH,Ruan XM.Comparation of paeoniflorin and ferulic acid between single and mixed decoction of Buyanghuanwu decoction[J].Beijing J Tradit Chin Med(北京中医药),2008,27(8):643-645.
    [7] Song X,Tao CL,Meng GD,et al.HPLC - DAD detection of Danggui-Shaoyao powder main chemical components[J].J Anhui Tradit Chin Med(安徽中医学院学报),2012,31(1):65-68.
    [8] Zhou Y,Tao CL,Xu F,et al.Optimization of extraction technology for Danggui-Shaoyao powder by multiple-index comprehensive scoring method[J].Chin J Exp Tradit Med Form(中国实验方剂学杂志),2012,18(19):20-23.
计量
  • 文章访问数:  1392
  • HTML全文浏览量:  0
  • PDF下载量:  2026
  • 被引次数: 0
出版历程
  • 刊出日期:  2014-04-24

目录

    /

    返回文章
    返回
    x 关闭 永久关闭