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四氢小檗碱的拆分

Resolution of Tetrahydroberberine

  • 摘要: 目的 通过化学拆分得到四氢小檗碱的光学异构体。方法 四氢小檗碱由小檗碱制备,以(-)/( )二对甲苯甲酰酒石酸为拆分剂对其进行拆分。结果 拆分所得的(-)/( )四氢小檗碱旋光值与文献报道一致。结论 通过化学拆分成功地获得了(-)/( )四氢小檗碱。

     

    Abstract: AIM The purpose is to resolute tetrahydroberberine.METHODS Tetrahydroberberine was synthesized from berberine chloride,then resoluted with (+) /(-) di - o,o,-p -toluyl-tartaric acid which was prepared from D/L -tartaric acid.RESULTS AND CONCLUTION S

     

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