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银杏叶中一个新的萜内酯类成分(英文)

A new ginkgolide from Ginkgo biloba

  • 摘要: 目的 : 研究银杏(Ginkgo biloba L.)叶中新的化学成分。 方法 : 运用柱色谱方法分离纯化,利用UV、IR、MS、1H NMR、13C NMR等色谱技术鉴定化合物结构。 结果 : 从银杏叶中分离鉴定出1个新化合物:1,7,10-三羟基-3,14-去氢银杏内酯(Ⅱ)和1个已知化合物:银杏内酯L(ginkgolide L)(Ⅰ)。 结论 : 化合物Ⅱ为新化合物,命名为银杏内酯N(ginkgolide N);化合物Ⅰ的光谱数据为首次报道。

     

    Abstract: Aim :To study new chemical constituents of the leaves of Ginkgo biloba L. Methods :Isolation and purification were carried out by several chromatographic methods.The structures of the compounds were elucidated by detailed analysis of their UV,IR,MS,1H NMR and 13C NMR spectra. Results :A new ginkgolide,ginkgolide N(1,7,10-trihydroxy-3,14- dehydroginkgolide,II),along with a known compound,was isolated from the leaves of G.biloba.The structure of the known one was elucidated as ginkgolide L(I). Conclusion :Compound II was a new compound.The complete spectroscopic data of compound I were reported for the first time.

     

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