Citation: | LI Lili, WANG Hongpeng, TIAN Haiwei, LI Jin, GAO Shuangshuang, HA Jing. Determination of 6 residual solvents in selexipag by headspace gas chromatography[J]. Journal of China Pharmaceutical University, 2018, 49(1): 93-96. DOI: 10.11665/j.issn.1000-5048.20180113 |
[1] |
Liu YG,Zhao LJ,Xiao GZ,et al.Selexipag[J].Drugs Clin(现代药物与临床),2010,25(6):469-471.
|
[2] |
Du C,Liu YX.Selexipag[J].Chin J Med Chem(中国药物化学杂志),2016,26(4):352.
|
[3] |
Xia XM.FDA approved Uptarvi(selexipag)tablets in the treatment of pulmonary arterial hypertension[J].J Guangdong Pharm Univ(广东药学院学报),2016,32(1):35.
|
[4] |
Wang H.Study on the synthesis of selexipag(Selexipag的工艺研究)[D].Shijiazhuang:Hebei University of Science and Technology,2017.
|
[5] |
Shang ZH,Wang H,Fang Q.Method for preparing selexipag:CN,201610357729.3[P].2016-06-20[2017-07-15] .
|
[6] |
Chinese Pharmacopoeia Commission.Chinese Pharmacopoeia:part 4[S].(中华人民共和国药典:四部),Beijing:China Medical Science Press,2015:105-109.
|
[7] |
Ito Y,Ishizuki K,Sekiguchi W,et al.Analysis of residual solvents in annatto extracts using a static headspace gas chromatography method[J].Ameri J Analy Chem,2012,3(9):638-645.
|
[8] |
Teglia CM,Montemurro M,Zan MMD,et al.Multiple responses optimization in the development of a headspace gas chromatography method for the determination of residual solvents in pharmaceuticals[J].J Pharm Anal,2015,5(5):296-306.
|
[9] |
Grodowska K,Parczewski A.Grouping of residual solvents present in pharmaceuticals using experimental planning and chemometric methods[J].Acta Poloniae Pharm,2013,70(2):191-203.
|
[10] |
Cheng C,Liu S,Mueller B J,et al.A generic static headspace gas chromatography method for determination of residual solvents in drug substance[J].J Chromatogr A,2010,1217(41):6413-6421.
|
[11] |
Huang R,Zhang SJ,Huang LY.Determination of residual organic solvents in fenazinel dihydrochloride by headspace gas chromatography[J].J China Pharm Univ(中国药科大学学报),2008,39(2):183-184.
|
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