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LIU Xiao-rong, YOU Qi-dong, WANG Jin-xin. Tandem Claisen rearrangement/Diels-Alder reaction in ionic liquid[J]. Journal of China Pharmaceutical University, 2009, 40(6): 481-485.
Citation: LIU Xiao-rong, YOU Qi-dong, WANG Jin-xin. Tandem Claisen rearrangement/Diels-Alder reaction in ionic liquid[J]. Journal of China Pharmaceutical University, 2009, 40(6): 481-485.
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Tandem Claisen rearrangement/Diels-Alder reaction in ionic liquid

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  • Aim ：The tandem Claisen rearrangement/Diels-Alder reaction in ionic liquid was carried out to find better changes for the conversion. Methods ：The synthesis started with replaced benzoic acid via acylation，cyclization，demethylation，allylation and then tandem Claisen rearrangement/Diels-Alder reaction in trational solvent and ionic liquid separately. Results ：BmimBF4 raised the yield of the target compound and shortened the reaction time compared with the traditional solvent. Conclusion ：BmimBF4 can promote the tandem Claisen rearrangement/Diels-Alder reaction.
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